Bruker AC/AM User's Guide (BUG)

The Chemistry Department and University will not accept responsibility for any problems arising from the inadvertent inaccuracies and mistakes that are contained in this User Guide.
Please let me know when you find mistakes.

This User Guide may be distributed freely with proper acknowledgements. It may not be used for any commercial activities.

Copyright © 1994-2014 Charles G. Fry:
All Rights Reserved. Last updated May 13, 2010.

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Step-by-Step Intro for Athena

BUG Table of Contents

    1. Title page, Detailed Table of Contents, and
      Facility Description

    2. Bruker AC Acquisition Basics
      Pulse Sequence Description; Deuterium Lock; Shimming; Acquisition Parameters
    3. Introduction to AC+ Spectrometers
      Locking and Shimming with the SCM; Job Files and Lock Power; Data Collection;
      File Transfer: NMRLINK; Departure; Adjusting for SW and O1;
      Spectra Showing Folding of Deshielded Proton; Caveats

    4. Primers for Areas of Common Interest
    5. AM/AC Spectrometer Software
      ADAKOS (Aspect Disk And Keyboard Operating System)
        Control Keys and System Commands; Files in DISNMR
        Common Acquisition Commands
        Common Pulse Sequence Commands and Parameters
        Common Data Processing Commands; Common EP Commands
      Plotting with DISNMR
    6. 2nd Order Shimming and High Resolution Check-Out
      2nd Order Lock Shimming (Match Tuning) on Z2;
      High Resolution Check-Out:
        FID shimming; window set-up and acquisition;
        lorentzian to gaussian line shape transformation
        resolution enhancement
    7. Saving Group-Specific Jobfiles, Shim Files, etc.
    8. Variable Temperature Measurements
    9. HOMODEC on AM/AC Spectrometers
    10. 1H Spin-Lattice Relaxation, T1
    11. 1D NOE Measurements
    12. Homonuclear COSY
    13. 31P and 19F Measurments on Athena (C636 HW handout)
    14. X-Nucleus Decoupling on Athena (AC-300a)
    15. Heteronuclear Correlation on AM/AC Consoles
    16. NOESY
    17. Polarization Transfer Experiments (INEPT and DEPT)
    18. AM/AC Automation Sequence Listings


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Copyright © 1996-2014
All Rights Reserved. Last updated Feb 27, 2014.